HuagongsheHuagongshe Chemistry Print Report · For research reference only
Imidazo(1,2-a)pyridine → HCID 19925050, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Imidazo(1,2-a)pyridine | HCID 78960 | — |
| Reactant | N-[3-(Bromomethyl)phenyl]-4-(tetradecyloxy)-benzeneacetamide | HCID 10052253 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 19925050 | HCID 19925050 | 81.4% |
Reaction Steps
A mixture of 1.5 g of N-[3-(bromomethyl)phenyl]-4-(tetradecyloxy)benzeneacetamide and 1.03 g of imidazo[1,2-a]pyridine in 25 ml of acetonitrile is refluxed under argon for 3.5 hours. The solvent is evaporated and the residue stirred with ether and collected by centrifugation. The solid is washed several times with ether and vacuum dried to give 1.5 g of the desired product as a white powder, m.p. 133°-135° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05128351 |
| Source dataset | uspto-grants-1992_07 |
| ORD ID | ord-b8a525a6a78b4c29a765c6fb7c3c9a96 |
| Source note | uspto-grants-1992_07 |