HuagongsheHuagongshe Chemistry Print Report · For research reference only
Heptane → Toluene heptane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Heptane | HCID 8900 | — |
| Reactant | 2,4-Dibromophenol | HCID 12005 | — |
| Reactant | Phenol, 2,4-dibromo-, phosphate (3:1) | HCID 14670658 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | Toluene heptane | HCID 22263336 | — |
Reaction Steps
Two hundred and eighty-four grams of crude tris-(2,4-dibromophenyl)phosphate were mixed with 808 grams of a solution of 85% n-heptane and 15% toluene as above. The liquid portion weighed 733 grams and contained 0.047% 2,4-dibromophenol, 1.45% ester product and 0.06% chloridates.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05128496 |
| Source dataset | uspto-grants-1992_07 |
| ORD ID | ord-555e4b438369405a8d9ce68fee2899ca |
| Source note | uspto-grants-1992_07 |