HCID 66577150, compound → {2-Butyl-4-chloro-1-[(4-nitrophenyl)methyl]-1H-imidazol-5-yl}acetic acid

Participants

Reaction Steps

Methyl 2-butyl-5-chloro-1-(4-nitrobenzyl)-imidazole-5-acetate was also prepared by the procedure described in Example 2Part B from 2-butyl-5-chloro-1-(4-nitrobenzyl)imidazole-5-acetic acid. NMR (200 MHz, CDCl3) δ 8.23 (d, 2H, J=10Hz); 7.20 (d, 2H, J=10Hz); 5.21 (s, 2H); 3.75 (s, 3H); 3.67 (s, 2H); 2.58 (t of t, 2H, J=7Hz); 1.32 (q of t, 2, J=7Hz); 0.86 (t, 3H, J=7Hz). Mass Calcd. for C17H20ClN3O4 ; 365.1142. Found 365.1132.

Provenance & Evidence