HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4,6-Triisopropylbenzenesulfonyl azide → 4-Benzyl-1,3-oxazolidin-2-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4,6-Triisopropylbenzenesulfonyl azide | HCID 371707 | — |
| Reactant | 3-[3-Cyclopentyl-1-oxopropyl]-4-(phenylmethyl)-2-oxazolidinone | HCID 4712668 | — |
| Product | 4-Benzyl-1,3-oxazolidin-2-one | HCID 559668 | — |
Reaction Steps
Following the procedure described in Example 46 for the preparation of the corresponding cyclooctyl derivative, 2.1 g of S)-3-[3-cyclopentyl-1-oxopropyl]-4-(phenylmethyl)-2-oxazolidinone and 2.5 g of 2,4,6-triisopropylbenzenesulfonyl azide yielded 1.23 g of [4S-3-(2S)]-3-[2-azido-3-cyclopentyl)-1-oxopropyl]-4-(phenylmethyl)-2-oxazolidinone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05128448 |
| Source dataset | uspto-grants-1992_07 |
| ORD ID | ord-2bb88379bc8241e7b739a209062f380d |
| Source note | uspto-grants-1992_07 |