HRID65397

反应详情

EQUATION

反应方程式

HRID 65397 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A suspension of 1.50 g. of 1,4-bis[2-(2-hydroxyethylamino)ethylamino]-5,8-dihydroxyanthraquinone in 75 ml. of ethyl triflouroacetate and 75 ml. of methanol is stirred for 10 minutes. Evaporation of the resulting solution in vacuo at 30° C. leaves a residue which is washed and macerated with methylene chloride, giving 2.11 g. of blue-black solid, m.p. 162° C.

WORKUP

后处理

  1. additionA suspension of 1.50 g
  2. customEvaporation of the resulting solution in vacuo at 30° C.
  3. customleaves a residue which
  4. washis washed
  5. customgiving 2.11 g