HCID 19888400, compound → HCID 19888386, compound

HRID 654091Notes

Reaction equation

HRID 654091 reaction equation
[CH2:1]([N:3]1[CH2:6][CH:5]([O:7][C:8]2[CH:13]=[CH:12][C:11]([N+:14]([O-])=O)=[CH:10][CH:9]=2)[CH2:4]1)[CH3:2]>C(O)C.[Pd]>[NH2:14][C:11]1[CH:12]=[CH:13][C:8]([O:7][CH:5]2[CH2:4][N:3]([CH2:1][CH3:2])[CH2:6]2)=[CH:9][CH:10]=1

Participants

4

Reactant 1

HCID 19888400HCID 19888400, compound

Product 1

HCID 19888386HCID 19888386, compound

Reagents, catalysts & solvents 2

HCID 23938PalladiumCatalystHCID 702EthanolSolvent

Procedure

A solution of 1-ethyl-3-(4-nitrophenoxy)azetidine in ethanol is subjected to catalytic reduction using palladium on carbon catalyst using standard procedures to obtain the title compound.

Sources & evidence

ORD record
ord-169521eb724d4e2cb5569b26de5d60b0
Source dataset
uspto-grants-1992_07
Patent number
US05130309

Reaction notes

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