HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 19774697, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Ethanethiol | HCID 6343 | — |
| Reactant | HCID 19774688 | HCID 19774688 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 19774697 | HCID 19774697 | — |
Reaction Steps
19.3 g (0.1 mol) of 3,5-dioxo-4-propionylcyclohexanecarbonitrile and 6.5 g (0.105 mol) of ethyl mercaptan were dissolved in 800 ml of dry diethyl ether and reacted with hydrogen chloride as described in Example 2.1: 20.7 g (71% of theory) of compound 2.2 [melting point 180°-185° C. (decomposition)].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05130453 |
| Source dataset | uspto-grants-1992_07 |
| ORD ID | ord-6607dc27cca94492969587e8f57a14b0 |
| Source note | uspto-grants-1992_07 |