HCID 54003692, compound → HCID 19888973, compound

Participants

Reaction Steps

To CH2Cl2 was added the benzyl alcohol (22 g) from Step B, above and then pyridinium chlorochromate (30.75 g; 0.15 mmol). The reaction mixture was stirred at room temperature for 2 hours then filtered and concentrated to afford 12.0 g of the subtitle compound. Several lots of the subtitle compound were prepared according to the procedures of Step A, B, and C, and were combined to afford 35.2 g of the subtitle compound.

Provenance & Evidence