1-Methoxy-4-nitro-3-(2-nitroethenyl)-2-(phenylmethoxy)benzene → HCID 18962537, compound

HRID 654381Notes

Reaction equation

HRID 654381 reaction equation
C(OC1C2OC=2C=C([N+]([O-])=O)C=1C=C[N+]([O-])=O)C1C=CC=CC=1.[CH2:24]([O:31][C:32]1[C:42]([O:43][CH3:44])=[CH:41][CH:40]=[C:39]([N+:45]([O-])=O)[C:33]=1[CH:34]=[CH:35][N+]([O-])=O)[C:25]1[CH:30]=[CH:29][CH:28]=[CH:27][CH:26]=1>>[CH2:24]([O:31][C:32]1[C:42]([O:43][CH3:44])=[CH:41][CH:40]=[C:39]2[C:33]=1[CH:34]=[CH:35][NH:45]2)[C:25]1[CH:26]=[CH:27][CH:28]=[CH:29][CH:30]=1

Participants

3

Reactant 2

HCID 538011151-Methoxy-4-nitro-3-(2-nitroethenyl)-2-(phenylmethoxy)benzeneHCID 86745996HCID 86745996, compound

Product 1

HCID 18962537HCID 18962537, compoundYield 86%

Procedure

This compound is obtained according to the operating method described in Example 1c, in which the 2-benzyloxy-3-epoxy-6,β-dinitrostyrene is replaced with 2-benzyloxy-3-methoxy-6,β-dinitrostyrene. A white powder (yield=86%, m.p.=83°-84° C.) is obtained.

Workup

  1. customThis compound is obtained

Sources & evidence

ORD record
ord-8c607d35fcff421595538fb49d6da6b3
Source dataset
uspto-grants-1992_07
Patent number
US05131911

Reaction notes

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