HCID 14208511, compound → HCID 57112142, compound

HRID 654383Notes

Reaction equation

HRID 654383 reaction equation
[CH2:1]([O:8][C:9]1[C:16]([O:17][CH2:18]C)=[CH:15][CH:14]=[C:13]([N+]([O-])=O)[C:10]=1[CH:11]=O)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.C(OC1C(OC)=CC=[C:35]([N+:41]([O-:43])=[O:42])[C:32]=1C=O)C1C=CC=CC=1>>[CH2:1]([O:8][C:9]1[C:16]([O:17][CH3:18])=[CH:15][CH:14]=[C:13]([CH2:35][N+:41]([O-:43])=[O:42])[C:10]=1[CH:11]=[CH:32][CH2:35][N+:41]([O-:43])=[O:42])[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

Participants

3

Reactant 2

HCID 14208511HCID 14208511, compoundHCID 18962559HCID 18962559, compound

Product 1

HCID 57112142HCID 57112142, compoundYield 53%

Procedure

This compound is obtained according to the operating method described in Example 2a, in which the 2-benzyloxy-3-ethoxy-6-nitrobenzaldehyde is replaced with 2-benzyloxy-3-methoxy-6-nitrobenzaldehyde. A light yellow powder (yield=53%, m.p.=149°-150° C.) is obtained.

Workup

  1. customThis compound is obtained

Sources & evidence

ORD record
ord-6ed4976ddcbb4fad875e04d5a7998cbe
Source dataset
uspto-grants-1992_07
Patent number
US05131911

Reaction notes

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