HCID 57070113, compound → HCID 18962534, compound

HRID 654384Notes

Reaction equation

HRID 654384 reaction equation
[CH2:1]([O:8][C:9]1[C:20]([O:21][CH2:22]C)=[CH:19][CH:18]=[C:17](C[N+]([O-])=O)[C:10]=1[CH:11]=[CH:12][CH2:13][N+]([O-])=O)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.C(OC1C(OC)=CC=C(C[N+]([O-])=O)C=1C=CC[N+:41]([O-])=O)C1C=CC=CC=1>>[CH2:1]([O:8][C:9]1[C:20]([O:21][CH3:22])=[CH:19][CH:18]=[C:17]2[C:10]=1[CH:11]=[C:12]([CH3:13])[NH:41]2)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 57070113HCID 57070113, compoundHCID 57112142HCID 57112142, compound

Product 1

HCID 18962534HCID 18962534, compoundYield 40%

Procedure

This compound is obtained according to the operating method described in Example 2b, in which the 2-benzyloxy-3-ethoxy-6,β-dinitromethylstyrene is replaced with 2-benzyloxy-3-methoxy-6,β-dinitromethylstyrene. A pale yellow powder (yield=40%, m.p.=74°-75° C.) is obtained.

Workup

  1. customThis compound is obtained

Sources & evidence

ORD record
ord-bcd0dc8027a74f5b9c7ceb0cb0e88493
Source dataset
uspto-grants-1992_07
Patent number
US05131911

Reaction notes

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