Formic Acid → HCID 14819422, compound

HRID 654441Notes

Reaction equation

HRID 654441 reaction equation
[CH3:1][C:2]1([CH3:21])[CH:11]([OH:12])[CH:10]([N:13]2[CH:18]=[CH:17][CH:16]=[CH:15][C:14]2=[O:19])[C:9]2[C:4](=[CH:5][CH:6]=[C:7]([NH2:20])[CH:8]=2)[CH2:3]1.[CH:22](O)=[O:23]>N1C=CC=CC=1>[CH3:1][C:2]1([CH3:21])[CH:11]([OH:12])[CH:10]([N:13]2[CH:18]=[CH:17][CH:16]=[CH:15][C:14]2=[O:19])[C:9]2[C:4](=[CH:5][CH:6]=[C:7]([NH:20][CH:22]=[O:23])[CH:8]=2)[CH2:3]1

Participants

4

Reactant 2

HCID 284Formic AcidHCID 14819421HCID 14819421, compound

Product 1

HCID 14819422HCID 14819422, compound

Reagents, catalysts & solvents 1

HCID 1049PyridineSolvent

Procedure

A solution of 1 g of 2,2-dimethyl-4-(2-oxo-1,2-dihydro-1-pyridyl)-6-amino-1,2,3,4-tetrahydro-3-naphthol in 15 ml of formic acid and 1 ml of pyridine is boiled for 16 hours and evaporated. Working up in the customary manner gives 2,2-dimethyl-4-(2-oxo-1,2-dihydro-1-pyridyl)-6-formamido-1,2,3,4-tetrahydro-3-naphthol.

Workup

  1. customevaporated

Sources & evidence

ORD record
ord-4a01cb52eac440a6b9943be136bc22f2
Source dataset
uspto-grants-1992_07
Patent number
US05132307

Reaction notes

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