HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
HRID 654459Erstellt: 25. Oktober 2026
5-Chloro-2-nitrobenzoic acid → 5-Chloro-2-nitrobenzoyl chloride
https://huagongshe.com/reaction/654459
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|
| Edukt | 5-Chloro-2-nitrobenzoic acid | HCID 17286 | — |
| Edukt | Thionyl Chloride | HCID 24386 | — |
| Produkt | 5-Chloro-2-nitrobenzoyl chloride | HCID 2723685 | — |
Reaktionsschritte
A mixture of 80.6 g of 5-chloro-2-nitrobenzoic acid and 58.2 ml of thionyl chloride is heated at 90° C. for 2 hours. The excess thionyl chloride is then distilled off in vacuo. 87.1 g of 5-chloro-2-nitrobenzoyl chloride are obtained.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patentnummer | US05132314 |
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| Quelldatensatz | uspto-grants-1992_07 |
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| ORD ID | ord-a77377dc679e46d883508eddd15de74a |
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| Quellennotiz | uspto-grants-1992_07 |
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