HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 85657722, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Hydroxyamine hydrochloride | HCID 443297 | — |
| Reactant | (3-Benzyl-1H-indol-1-yl)acetaldehyde | HCID 54560454 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 85657722 | HCID 85657722 | — |
Reaction Steps
To a solution of the aldehyde from Step 2 (390 mg, 1.57 mmol) in EtOH (6 mL) there was added hydroxylamine hydrochloride (435 mg, 6.26 mmol), then pyridine (3 mL). The mixture was stirred at r.t. for 45 minutes, then it was evaporated to dryness. The residue was partitioned between Et2O and H2O, and by evaporation of the ethereal fraction the title oxime was obtained as a soft solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05132319 |
| Source dataset | uspto-grants-1992_07 |
| ORD ID | ord-10c2bd2ce5a84d868574ac490eda6723 |
| Source note | uspto-grants-1992_07 |