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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 654541Generated: October 29, 2026

HCID 10452275, compound → HCID 10090968, compound

https://huagongshe.com/reaction/654541

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 10452275HCID 10452275—
SolventDimethyl SulfoxideHCID 679—
ProductHCID 10090968HCID 1009096849.9%

Reaction Steps

In a manner similiar to Scheme I, 16 (43.5 g, 0.115 mol) was treated with sulfur trioxide pyridine complex (56.0 g, 0.345 mol) in anhydrous DMSO and workup provided 21.6 g of brown oil which was taken forward without additional purification.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05132312
Source datasetuspto-grants-1992_07
ORD IDord-a44f532db6ec44129e7e5b0ab67c00d0
Source noteuspto-grants-1992_07