HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrabutylammonium Fluoride → HCID 87845477, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrabutylammonium Fluoride | HCID 2724141 | — |
| Reactant | HCID 131716812 | HCID 131716812 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 87845477 | HCID 87845477 | 74.9% |
Reaction Steps
In a manner similar to Scheme V, 38 (0.20 gm) was treated with tetrabutylammonium fluoride in THF and acetic acid and, after workup, purified by SiO2 using 1:1 hexanes:EtOAc as eluent and yielded 0.101 g of product. mp 73°-5° C. Anal. C29H32FNO5 : Theory C: 70.57; H: 6.54; N:2.84. Found C: 70.37; H: 6.94; N: 3.06.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05132312 |
| Source dataset | uspto-grants-1992_07 |
| ORD ID | ord-b2fe594b278842d1b5fd77205bb12f03 |
| Source note | uspto-grants-1992_07 |