HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diazomethane → HCID 19769486, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diazomethane | HCID 9550 | — |
| Reactant | HCID 10470291 | HCID 10470291 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 19769486 | HCID 19769486 | — |
Reaction Steps
A solution of diazomethane in diethyl ether was added to a solution of (-)-2-(3-benzyloxy-5-fluorophenyl)-2-hydroxybutyric acid (2.24 g) in diethyl ether (35 ml) until the reaction mixture retained a yellow colouration. The mixture was evaporated to give methyl (-)-2-(3-benzyloxy-5-fluorophenyl)-2-hydroxybutyrate (2.27 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05132328 |
| Source dataset | uspto-grants-1992_07 |
| ORD ID | ord-fd4505572cbc417eb7e577b2988470de |
| Source note | uspto-grants-1992_07 |