2,4-Di-tert-butylphenol → HCID 19742179, compound

HRID 654633Notes

Reaction equation

HRID 654633 reaction equation
[CH2:1]([N:8]1[C:12]2([CH2:17][O:16][P:15](OC3C=CC=CC=3)[O:14][CH2:13]2)[CH2:11][O:10][P:9]1[O:25][C:26]1[CH:31]=[CH:30][CH:29]=[CH:28][CH:27]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[C:32]([C:36]1[CH:41]=[C:40]([C:42]([CH3:45])([CH3:44])[CH3:43])[CH:39]=[CH:38][C:37]=1[OH:46])([CH3:35])([CH3:34])[CH3:33].C[O-].[Na+]>>[CH2:1]([N:8]1[C:12]2([CH2:17][O:16][P:15]([O:46][C:37]3[CH:38]=[CH:39][C:40]([C:42]([CH3:45])([CH3:44])[CH3:43])=[CH:41][C:36]=3[C:32]([CH3:35])([CH3:34])[CH3:33])[O:14][CH2:13]2)[CH2:11][O:10][P:9]1[O:25][C:26]1[CH:27]=[CH:28][C:29]([C:2]([CH3:7])([CH3:3])[CH3:1])=[CH:30][C:31]=1[C:12]([CH3:17])([CH3:13])[CH3:11])[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

Participants

4

Reactant 3

HCID 73112,4-Di-tert-butylphenolHCID 10942334Sodium MethoxideHCID 19742187HCID 19742187, compound

Product 1

HCID 19742179HCID 19742179, compound

Procedure

The product of Example 18 is reacted with two equivalents of 2,4-di-tert-butylphenol and sodium methoxide at reduced pressure and at an elevated temperature to afford the title compound.

Sources & evidence

ORD record
ord-2832e6d347b447fd9571800fe6fbce28
Source dataset
uspto-grants-1992_07
Patent number
US05132426

Reaction notes

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