HCID 14986463, compound → HCID 14986464, compound

HRID 654696Notes

Reaction equation

HRID 654696 reaction equation
C([O:8][C:9]1[C:18]2[C:13](=[CH:14][CH:15]=[CH:16][C:17]=2[CH3:19])[CH:12]=[CH:11][C:10]=1[C:20]([CH3:22])=[CH2:21])C1C=CC=CC=1>[C].[Pd].C(O)C>[CH:20]([C:10]1[CH:11]=[CH:12][C:13]2[C:18](=[C:17]([CH3:19])[CH:16]=[CH:15][CH:14]=2)[C:9]=1[OH:8])([CH3:22])[CH3:21]

Participants

4

Reactant 1

HCID 14986463HCID 14986463, compound

Product 1

HCID 14986464HCID 14986464, compoundYield 93.6%

Reagents, catalysts & solvents 2

HCID 178418390HCID 178418390, compoundCatalystHCID 702EthanolSolvent

Procedure

1.0 g of 1-benzyloxy-2-isopropenyl-8-methylnaphthalene and 0.1 g of 10% palladium-carbon (water content of 50%) were added to 40 ml of ethanol and hydrogenated at normal temperatures and normal pressures. The palladium-carbon was filtered through Celite, after which the filtrate was concentrated under reduced pressure to obtain 0.65 g of the captioned compound as a black oily substance.

Workup

  1. filtrationThe palladium-carbon was filtered through Celite
  2. concentrationafter which the filtrate was concentrated under reduced pressure

Sources & evidence

ORD record
ord-a9a9cf0dd173438bafabbccde08ceae4
Source dataset
uspto-grants-1992_07
Patent number
US05134111

Reaction notes

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