HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuric Acid → HCID 54209808, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | 4-Chlorobenzaldehyde | HCID 7726 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 4,4-Dimethylpentanal | HCID 11062343 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 54209808 | HCID 54209808 | — |
Reaction Steps
134 g (0.95 mol) of 4-chlorobenzaldehyde are added to a solution of 15.8 g of 50% strength sodium hydroxide solution in 500 ml of methanol, after which 90 g (0.79 mol) of 4,4-dimethylpentanal are added dropwise at 35° C. in the course of 3 hours. Stirring is carried out for three hours, after which the mixture is neutralized with dilute sulfuric acid and evaporated down and the residue is distilled.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05134167 |
| Source dataset | uspto-grants-1992_07 |
| ORD ID | ord-719a81354bc94aa894acb55445626916 |
| Source note | uspto-grants-1992_07 |