HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methacrylic Acid → Ethyl prop-2-enoate--methyl 2-methylprop-2-enoate (1/1)
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methacrylic Acid | HCID 4093 | — |
| Reactant | Methyl Methacrylate | HCID 6658 | — |
| Reactant | Benzoyl Peroxide | HCID 7187 | — |
| Reactant | Ethyl Acrylate | HCID 8821 | — |
| Reactant | Azane;hydrate | HCID 12896473 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | Ethyl prop-2-enoate--methyl 2-methylprop-2-enoate (1/1) | HCID 62704 | — |
Reaction Steps
To 150 g of isopropanol were added 55 g of ethyl acrylate, 35 g of methyl methacrylate and 10 g of methacrylic acid. To the resulting mixture was added 0.5 g of benzoyl peroxide, and thereafter, the mixture thus-obtained was subjected to polymerization reaction at 80° C. for 7 hours. Subsequently, 200 g of water and 4 g of 28% ammonia water were added thereto, and then, the isopropanol was completely removed by distillation to obtain an ethyl acrylate/methyl methacrylate copolymer.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05134189 |
| Source dataset | uspto-grants-1992_07 |
| ORD ID | ord-1334f21ecacd496b96c85f1ba489d456 |
| Source note | uspto-grants-1992_07 |