HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-(1-Naphthyl)-4-pentyn-1-ol → 5-(Naphth-1-yl)pentanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-(1-Naphthyl)-4-pentyn-1-ol | HCID 19955557 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | 5-(Naphth-1-yl)pentanol | HCID 10353200 | — |
Reaction Steps
A mixture of 5-(1-naphthyl)-4-pentyn-1-ol (500 ng, 2.37 mmol) and 5% palladium on barium sulfate (5 mg) in ethyl ether (30 ml) was stirred at room temperature under a hydrogen atmosphere for two days. Solvent removal, after filtration through celite, gave the title compound as a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05134128 |
| Source dataset | uspto-grants-1992_07 |
| ORD ID | ord-fc1489072aa34dfd8d39a00b9d7dfcbb |
| Source note | uspto-grants-1992_07 |