Dodecanoyl chloride → HCID 19885924, compound

Participants

Reaction Steps

4-(1,2-Dihydroxyethyl)-2-triethylsilylfuran (prepared by the procedure of Example 1 using 5-triethylsilyl-3-furaldehyde in place of the corresponding trimethylsilyl furaldehyde and preparing the 5-triethylsilyl-3-furaldehyde by the alternative procedure using triethylsilyl Chloride) is reacted with dodecanoyl chloride in the presence of triethylamine to give 4-(1-hydroxy-2-tridecanoyloxyethyl)-2-triethylsilylfuran. Treating this 1-hydroxy compound with acetic anhydride and pyridine gives 4-(1-acetoxy-2-tridecanoyl-oxyethyl)-2-triethylsilylfuran.

Provenance & Evidence