反应详情

温度

80 °C

In a 100 ml apparatus, there were combined 14.2 g (0.15 mol) of Me2SiHCl and 13.6 g (0.15 mol) of methallyl chloride, followed by 0.05 ml Pt catalyst solution at 21° C. Gentle heating caused a smooth exothermic reaction to 90° C. in 16 in. Reaction was heated at 80° C. until completed (50 min). Vacuum distillation yielded 23.14 g (83.4%) of Me2SiClCH2CHMeCH2Cl.

1. temperatureGentle heating
2. customa smooth exothermic reaction to 90° C. in 16 in
3. customReaction
4. custom(50 min)
5. distillationVacuum distillation