HuagongsheHuagongshe Chemistry Print Report · For research reference only
Salicylaldehyde → HCID 15311954, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Salicylaldehyde | HCID 6998 | — |
| Reactant | Ethyl 3-(triphenyl-lambda~5~-phosphanylidene)propanoate | HCID 12607919 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 15311954 | HCID 15311954 | — |
Reaction Steps
To a solution of 75.0 g (carbethoxyethylidene)triphenyl phosphorane in 350 ml of toluene, 23.2 g of salicylaldehyde was dropped in at 20° C. while cooling in an ice-bath. After stirring at room temperature for 90 mn., the reaction mixture was diluted with toluene and washed to neutrality with water.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | USRE043006E1 |
| Source dataset | uspto-grants-2011_12 |
| ORD ID | ord-4bada835d65a4d73ba88e933bd63e29b |
| Source note | uspto-grants-2011_12 |