HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(3-Pyridyl)cyclohex-3-en-1-one ethylene acetal → 4-(3-Pyridyl)cyclohexanone ethylene acetal
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(3-Pyridyl)cyclohex-3-en-1-one ethylene acetal | HCID 20034903 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | 4-(3-Pyridyl)cyclohexanone ethylene acetal | HCID 57892550 | 99.3% |
Reaction Steps
A mixture of 4-(3-pyridyl)cyclohex-3-en-1-one ethylene acetal (4.80 g, 22.1 mmol) in EtOAc (50 mL) containing 10% Pd/C (458 mg) was hydrogenated under atmospheric pressure for 3 h. After filtration of the catalyst, the solution was concentrated in vacuo, to yield 4-(3-pyridyl)cyclohexanone ethylene acetal (4.81 g, 99%) as yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08071591B2 |
| Source dataset | uspto-grants-2011_12 |
| ORD ID | ord-aeafbf19eef1400b9856273dd5efa6b4 |
| Source note | uspto-grants-2011_12 |