HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 6-Chloronicotinoyl Chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 6-Chloronicotinic acid | HCID 79222 | — |
| Product | 6-Chloronicotinoyl Chloride | HCID 2782165 | — |
Reaction Steps
Starting from 250 g 6-chloro-nicotinic acid and 850 ml SOCl2, and using the working conditions as in Ex. 1a, there is obtained 243 g 6-chloronicotinoyl chloride, m.p. 49°-51° C.; b.p. 75° C./0,05 mm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04614833 |
| Source dataset | uspto-grants-1986_09 |
| ORD ID | ord-de7ca287cc5446df885d2e8bfcc67893 |
| Source note | uspto-grants-1986_09 |