HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1'-Carbonyldiimidazole → 5-Methyloxazolo[4,5-b]pyridin-2(3H)-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1'-Carbonyldiimidazole | HCID 68263 | — |
| Reactant | 2-Amino-6-methylpyridin-3-ol | HCID 88500 | — |
| Product | 5-Methyloxazolo[4,5-b]pyridin-2(3H)-one | HCID 10012075 | — |
Reaction Steps
Reaction of 2-amino-6-methylpyridin-3-ol with CDI (carbonyldiimidazole) in a corresponding manner to Example 1.2 gives the desired product; ESI: 151 (M+H), Rt=1.58 min (method B).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08071593B2 |
| Source dataset | uspto-grants-2011_12 |
| ORD ID | ord-92cadd072a9947ba9cc51852f3894439 |
| Source note | uspto-grants-2011_12 |