HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lithium borohydride → HCID 44612132, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lithium borohydride | HCID 4148881 | — |
| Reactant | HCID 59149858 | HCID 59149858 | — |
| Product | HCID 44612132 | HCID 44612132 | 27% |
Reaction Steps
In analogy to the procedure described in Example 2, (S)-2-[4-(3-chloro-phenyl-carbamoyl)-7-oxo-[1,4]diazepan-1-yl]-4-((S)-4-hydroxy-6-aza-spiro[2.5]oct-6-yl)-butyric acid methyl ester and lithium borohydride gave the title compound in 27% yield as an off-white powder. MS: 465.3 (MH+, 1Cl).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08071586B2 |
| Source dataset | uspto-grants-2011_12 |
| ORD ID | ord-30742516fbae45fab486cf203f0d1907 |
| Source note | uspto-grants-2011_12 |