HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 65566Generated: October 25, 2026
2-Methylbenzenesulfonic acid → 4-(Hexylthio)phenol
https://huagongshe.com/reaction/65566
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 2-Methylbenzenesulfonic acid | HCID 6925 | — |
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | 2-Methyl-1-pentene | HCID 12986 | — |
| Reactant | 4-Mercaptophenol | HCID 240147 | — |
| Solvent | Water | HCID 962 | — |
| Product | 4-(Hexylthio)phenol | HCID 20086310 | — |
Reaction Steps
A 4-(hexylthio)phenol was prepared as follows. In a one liter flask equipped with thermometer, stirring rod and water condenser was added 126 grams of 4-mercaptophenol and 7 grams of toluenesulfonic acid. The flask contents were heated to 60° C. and 93 grams of 2-methyl-1-pentene were added over a fifty minute period. The flask contents were neutralized with 9 grams of Na2CO3 in aqueous solution and decanted. The reaction product was stripped to a pot temperature of 80° C. at 20 millimeters of mercury. It weighed 216 grams.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04128530 |
|---|
| Source dataset | uspto-grants-1978_12 |
|---|
| ORD ID | ord-ab70397f3e6949cf95fb20215605e801 |
|---|
| Source note | uspto-grants-1978_12 |
|---|
