HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexene → HCID 66850696, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexene | HCID 8079 | — |
| Reactant | HCID 45444158 | HCID 45444158 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 66850696 | HCID 66850696 | 87.7% |
Reaction Steps
The mixture of 6 g of 2-nitro-5-(4-benzylpiperazin-1-yl)benzoic acid, 15 mL of cyclohexene and 3 g of Pd/C (10%) is heated under reflux conditions in 120 mL of ethanol for 6 hours. The hot reaction mixture is filtered through celite filter. The filtrate is evaporated to obtain 4.8 g of the title compound. m.p.: 242° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08071601B2 |
| Source dataset | uspto-grants-2011_12 |
| ORD ID | ord-290213fe3fc44603acd67d37e879660e |
| Source note | uspto-grants-2011_12 |