Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzamide, 3-nitro-N-(3-nitrophenyl)- → Benzamide, 3-amino-N-(3-aminophenyl)-
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzamide, 3-nitro-N-(3-nitrophenyl)- | HCID 66861 | — |
| 반응물 | HCID 178418361 | HCID 178418361 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 용매 | 1,4-Dioxane | HCID 31275 | — |
| 생성물 | Benzamide, 3-amino-N-(3-aminophenyl)- | HCID 66859 | — |
반응 단계
A solution of 14.3 g of 3,3'-dinitrobenzanilide in 150 ml. of dioxane is hydrogenated at three atmospheres of hydrogen using 1 g. of 10% palladium-on-charcoal catalyst. The catalyst is removed by filtration and the filtrate evaporated to dryness. The residue is recrystallized from ethanol. There is obtained 8.72 g. of material melting at 123°-4°.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04128570 |
| 출처 데이터셋 | uspto-grants-1978_12 |
| ORD ID | ord-4e2946f77f2c40ab8b38465e36dfb128 |
| 출처 메모 | uspto-grants-1978_12 |