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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 65610생성일: 2026년 10월 25일

Benzamide, 3-nitro-N-(3-nitrophenyl)- → Benzamide, 3-amino-N-(3-aminophenyl)-

https://huagongshe.com/reaction/65610

반응식

참여 물질

역할이름HCID투입량
반응물Benzamide, 3-nitro-N-(3-nitrophenyl)-HCID 66861—
반응물HCID 178418361HCID 178418361—
촉매PalladiumHCID 23938—
용매1,4-DioxaneHCID 31275—
생성물Benzamide, 3-amino-N-(3-aminophenyl)-HCID 66859—

반응 단계

A solution of 14.3 g of 3,3'-dinitrobenzanilide in 150 ml. of dioxane is hydrogenated at three atmospheres of hydrogen using 1 g. of 10% palladium-on-charcoal catalyst. The catalyst is removed by filtration and the filtrate evaporated to dryness. The residue is recrystallized from ethanol. There is obtained 8.72 g. of material melting at 123°-4°.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US04128570
출처 데이터셋uspto-grants-1978_12
ORD IDord-4e2946f77f2c40ab8b38465e36dfb128
출처 메모uspto-grants-1978_12