HRID656271

反应详情

EQUATION

反应方程式

HRID 656271 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

(2-Methanesulfonylaminophenyl)acetonitrile (300 mg) was mixed with 10% palladium/carbon (catalytic amount) in methanol (20 ml) and the mixture was stirred under hydrogen gas atmospheres for 48 hours. After confirming the completion of the reaction using TLC, the resulting mixture was filtered through celite and the filtrate was concentrated under reduced pressure. The following procedure was carried out using the concentrate which was not purified.

WORKUP

后处理

  1. filtrationthe resulting mixture was filtered through celite
  2. concentrationthe filtrate was concentrated under reduced pressure
  3. concentrationconcentrate which
  4. customwas not purified