12-Hydroxy-8-(methanesulfonyl)heptadecanoic acid → HCID 21317552, compound

HRID 65642Notes

Reaction equation

HRID 65642 reaction equation
[CH3:1][S:2]([CH:5]([CH2:15][CH2:16][CH2:17][CH:18]([OH:24])[CH2:19][CH2:20][CH2:21][CH2:22][CH3:23])[CH2:6][CH2:7][CH2:8][CH2:9]CCC(O)=O)(=[O:4])=[O:3].CSC(CCCC(O)CCCCC)CCCC[O:32][CH2:33][C:34]([OH:36])=[O:35]>>[CH3:1][S:2]([CH:5]([CH2:15][CH2:16][CH2:17][CH:18]([OH:24])[CH2:19][CH2:20][CH2:21][CH2:22][CH3:23])[CH2:6][CH2:7][CH2:8][CH2:9][O:32][CH2:33][C:34]([OH:36])=[O:35])(=[O:3])=[O:4]

Participants

3

Reactant 2

HCID 2021027912-Hydroxy-8-(methanesulfonyl)heptadecanoic acidHCID 213176335-Methylthio-9-hydroxytetradecyloxyacetic acid

Product 1

HCID 21317552HCID 21317552, compound

Procedure

This compound is prepared essentially by the method described in Example 2 except that the 8-methylthio-12-hydroxyheptadecanoic acid of Example 2 is replaced by 5-methylthio-9-hydroxytetradecyloxyacetic acid. The product is purified by chromatography on silica gel and is obtained as a very viscous yellowish oil.

Workup

  1. customThis compound is prepared essentially by the method
  2. customThe product is purified by chromatography on silica gel
  3. customis obtained as a very viscous yellowish oil

Sources & evidence

ORD record
ord-ac73e247c5a846ec93ffbbfd7f468cb7
Source dataset
uspto-grants-1978_12
Patent number
US04128564

Reaction notes

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