Sulfuric Acid → HCID 23200488, compound

HRID 656716Notes

Reaction equation

HRID 656716 reaction equation
S(=O)(=O)(O)O.[C:6]([CH2:13][OH:14])([C:9]([F:12])([F:11])[F:10])([F:8])[F:7].C[O:16][CH:17](O)[C:18]([F:21])([F:20])[F:19]>>[C:18]([CH:17]([O:14][CH2:13][C:6]([C:9]([F:12])([F:11])[F:10])([F:8])[F:7])[OH:16])([F:21])([F:20])[F:19]

Participants

4

Reactant 3

HCID 1118Sulfuric AcidHCID 98722,2,3,3,3-PentafluoropropanolHCID 98922,2,2-Trifluoro-1-methoxyethanol

Product 1

HCID 23200488HCID 23200488, compound

Procedure

This reaction was carried out in the same manner as described in Example 1 using charges of sulfuric acid (175 g), C2F5CH2OH (86.7 g, 0.578 mole) and trifluoroacetaldehyde methyl hemiacetal (Alfa Aesar, 50 g, 90% purity, 0.346 mole). The receiver gained 27.1 g in weight and this solution was used without purification in the next step.

Workup

  1. customthis solution was used without purification in the next step

Sources & evidence

ORD record
ord-b863c7735f864f9387d45a9ab1d5f774
Source dataset
uspto-grants-2011_12
Patent number
US08071816B2

Reaction notes

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