Sodium Acetate → HCID 68627573, compound

Participants

Reaction Steps

step 2—A solution of 36 (0.178 g, 0.267 mmol), PCC (0.114 g, 0.680 mmol), NaOAc (214 mg) and DCM (8 mL) was added stirred overnight. The solvent was evaporated and the crude product purified on a SiO2 column eluting with an EtOAc/hexane gradient (0 to 50% EtOAc) to afford 0.081 g of [3-({5-cyclopropyl-2-[4-(4-fluoro-phenoxy)-phenyl]-3-methylcarbamoyl-benzofuran-6-yl}-methanesulfonyl-amino)-2-oxo-propyl]-carbamic acid tert-butyl ester (38).

Provenance & Evidence