HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 12647858, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 15298916 | HCID 15298916 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 12647858 | HCID 12647858 | — |
Reaction Steps
A solution of 2-(2-tert-butoxy-2-oxoethyl)indane-2-carboxylic acid from Step B (1.50 g, 5.43 mmol) in EtOAc (100 mL) was saturated with HCl (g) and stood at ambient temperature for 1 h, then concentrated to dryness in vacuo, to give the title compound. MS: m/z=284 (M+Na+CH3 CN).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08071772B2 |
| Source dataset | uspto-grants-2011_12 |
| ORD ID | ord-df5c6db99124480baaf64aac180cb7cc |
| Source note | uspto-grants-2011_12 |