Furo[2,3-c]pyridin-5-ylmethanol → HCID 57423121, 화합물

HRID 656968노트

반응식

HRID 656968 반응식
[O:1]1[C:5]2=[CH:6][N:7]=[C:8]([CH2:10][OH:11])[CH:9]=[C:4]2[CH:3]=[CH:2]1>C(O)C.[Pd]>[O:1]1[C:5]2=[CH:6][N:7]=[C:8]([CH2:10][OH:11])[CH:9]=[C:4]2[CH2:3][CH2:2]1

참가 물질

4

반응물 1

HCID 22047174Furo[2,3-c]pyridin-5-ylmethanol

생성물 1

HCID 57423121HCID 57423121, 화합물

시약·촉매·용매 2

HCID 23938Palladium촉매HCID 702Ethanol용매

실험 절차

Furo[2,3-c]pyridin-5-ylmethanol (1.29 g, 8.7 mmol) was dissolved in ethanol (50 ml) and hydrogenated at rt, 1 atmosphere over 10% palladium on charcoal paste for 18 h. The mixture was filtered through kieselguhr and the filtrate evaporated to dryness, to give (1.31 g, 100%).

후처리

  1. filtrationThe mixture was filtered through kieselguhr
  2. customthe filtrate evaporated to dryness
  3. customto give (1.31 g, 100%)

출처 및 근거

ORD 기록
ord-f75907c016294692858f4de91dcc9f79
출처 데이터셋
uspto-grants-2011_12
특허 번호
US08071592B2

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