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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 657042Generated: October 31, 2026

HCID 86635341, compound → HCID 68994150, compound

https://huagongshe.com/reaction/657042

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 86635341HCID 86635341—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 68994150HCID 6899415096%

Reaction Steps

A solution of phenylmethyl ({(3R,4R)-1-[2-(7-fluoro-2-oxo-1(2H)-quinolinyl)ethyl]-4-hydroxy-3-pyrrolidinyl}methyl)carbamate (0.3 g) in dry methanol (15 mL) was treated with 10% Pd/C (0.08 g) and shaken under 15 psi at room temperature for 2 hours. The Pd catalyst was filtered through Celite®. The filtrate was evaporated to dryness to give an oil (0.2 g).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08071592B2
Source datasetuspto-grants-2011_12
ORD IDord-87d42e190cb34e3396cde5bfceb992b6
Source noteuspto-grants-2011_12