HuagongsheHuagongshe Chemistry Print Report · For research reference only
(3-methoxy-4-methylphenyl)methanol → 3-Methoxy-4-methylbenzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (3-methoxy-4-methylphenyl)methanol | HCID 11744818 | — |
| Catalyst | Manganese oxide | HCID 160959 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 3-Methoxy-4-methylbenzaldehyde | HCID 4715095 | — |
Reaction Steps
At ambient temperature, 36.35 g (238.8 mmol) of (3-methoxy-4-methylphenyl)-methanol and 207.6 g (2.4 moles/10 eq.) of manganese oxide are mixed into 730 mL of dichloromethane. Stirring is carried out at ambient temperature overnight, followed by filtration over Celite and rinsing with dichloromethane. After concentration of the combined filtrates, the desired product is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08076325B2 |
| Source dataset | uspto-grants-2011_12 |
| ORD ID | ord-96a21904e825421cb070c88fd0d19996 |
| Source note | uspto-grants-2011_12 |