HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromo-3-chloropropane → 4-(3-Chloropropoxy)-4'-methylbiphenyl
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromo-3-chloropropane | HCID 8006 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4-(4-Methylphenyl)phenol | HCID 1382789 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 4-(3-Chloropropoxy)-4'-methylbiphenyl | HCID 23150289 | — |
Reaction Steps
Following the procedure described in example 1§E, but starting from 4-hydroxy-4′-methylbiphenyl (194 mg), potassium carbonate (720 mg) and 1-bromo-3-chloropropane (517 μL) in N,N-dimethylformamide (1.5 mL) affords 274 g of 4-(3-chloropropoxy)-4′-methylbiphenyl.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08076329B2 |
| Source dataset | uspto-grants-2011_12 |
| ORD ID | ord-e1c702eafcb748e08c0afb386b2df57f |
| Source note | uspto-grants-2011_12 |