HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromo-3-chloropropane → 4'-Bromo-4-(3-chloropropoxy)biphenyl
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromo-3-chloropropane | HCID 8006 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 4-Bromo-4'-hydroxybiphenyl | HCID 95093 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | 4'-Bromo-4-(3-chloropropoxy)biphenyl | HCID 23150276 | 97.9% |
Reaction Steps
Following the procedure described in example 1§E, but starting from 4-bromo-4′-hydroxybiphenyl (5 g), potassium carbonate (13.8 g) and 1-bromo-3-chloropropane (15.7 g) in acetonitrile (100 mL) affords 6.4 g of 4′-bromo-4-(3-chloropropoxy)biphenyl as white crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08076329B2 |
| Source dataset | uspto-grants-2011_12 |
| ORD ID | ord-6d14d7c1247044628961cda114148a21 |
| Source note | uspto-grants-2011_12 |