HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalate → HCID 178521553, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalate | HCID 71081 | — |
| Reactant | HCID 23150285 | HCID 23150285 | — |
| Reactant | HCID 178461428 | HCID 178461428 | — |
| Product | HCID 178521553 | HCID 178521553 | 38% |
Reaction Steps
Reduction of 1-{3-[-4-(4-oxocyclohexyl)phenoxy]propyl}piperidine (1.57 g) as described for (3S)-1-{3-[trans-4-(4-hydroxycyclohexyl)phenoxy]propyl}-3-methyl-piperidine gives 600 mg of 1-{3-[trans-4-(4-hydroxycyclohexyl)phenoxy]-propyl}piperidine, oxalate as a white powder melting at 182° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08076329B2 |
| Source dataset | uspto-grants-2011_12 |
| ORD ID | ord-23c9ac35c11748ee98a71a3549df1772 |
| Source note | uspto-grants-2011_12 |