5-(Azidomethyl)-2-methylpyrimidine → (2-Methylpyrimidin-5-yl)methanamine

Beteiligte Stoffe

Reaktionsschritte

A mixture of 5-(azidomethyl)-2-methylpyrimidine (2.0, 13.4 mmol) in ethyl acetate (100 mL), and 10% Pd—C (4.0 g) was stirred under H2 (1 atm) for 1.5 hr. The catalyst was filtered off and filtrate was concentrated in vacuo to afford a white solid.

Herkunft & Nachweise