HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 58103573, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Ethanol | HCID 702 | — |
| Reactant | 1,4-Dioxane | HCID 31275 | — |
| Reactant | HCID 66872457 | HCID 66872457 | — |
| Product | HCID 58103573 | HCID 58103573 | — |
Reaction Steps
(R)—N—((R)-Cyclopropyl(6-(trifluoromethyl)pyridin-3-yl)methyl)-2-methylpropane-2-sulfinamide (0.245 g, 0.000765 mol), ethanol (2.7 g, 0.059 mol), and 4.0 M of hydrogen chloride in dioxane (2.7 mL, 0.011 mol) were combined and stirred overnight. Reaction was concentrated to down to oil and then redissolved and washed with ethanol for 3 times, and concentrated. The residue was dried on the high vacuum overnight to obtain the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08076345B2 |
| Source dataset | uspto-grants-2011_12 |
| ORD ID | ord-c4d40bef71e748109954805f1c147d3a |
| Source note | uspto-grants-2011_12 |