Acetonitrile → HCID 56833373, compound

HRID 657833Notes

Reaction equation

[CH3:1][C:2]([S:9][CH3:10])([CH3:8])[C:3]([O:5]CC)=O.[C:11](#[N:13])[CH3:12]>>[CH3:8][C:2]([S:9][CH3:10])([CH3:1])[C:3](=[O:5])[CH2:12][C:11]#[N:13]

Participants

Reactant 2

HCID 6342Acetonitrile

HCID 3016499Ethyl 2-methyl-2-(methylthio)propionate

Product 1

HCID 56833373HCID 56833373, compoundYield 81%

Procedure

The title compound was prepared from ethyl 2-methyl-2-(methylthio)propionate and acetonitrile, using a method similar to that of preparation 2, as a colourless oil in 81% yield.

Workup

customof preparation 2

Sources & evidence

ORD record: ord-3397b7c30d9747849a491ce671c07533
Source dataset: uspto-grants-2011_12
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08076356B2

Reaction notes

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