Pentanenitrile, 4,4-dimethyl-3-oxo- → HCID 58851621, compound

HRID 657847Notes

Reaction equation

HRID 657847 reaction equation
[CH3:1][C:2]([CH3:9])([CH3:8])[C:3](=O)[CH2:4][C:5]#[N:6].Cl.[CH2:11]([O:18][C:19]1[CH:24]=[CH:23][C:22]([NH:25][NH2:26])=[CH:21][CH:20]=1)[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1>>[CH2:11]([O:18][C:19]1[CH:20]=[CH:21][C:22]([N:25]2[C:5]([NH2:6])=[CH:4][C:3]([C:2]([CH3:9])([CH3:8])[CH3:1])=[N:26]2)=[CH:23][CH:24]=1)[C:12]1[CH:13]=[CH:14][CH:15]=[CH:16][CH:17]=1

Participants

3

Reactant 2

HCID 108871Pentanenitrile, 4,4-dimethyl-3-oxo-HCID 3016725(4-(Benzyloxy)phenyl)hydrazine monohydrochloride

Product 1

HCID 58851621HCID 58851621, compound

Procedure

The title compound was prepared from 4,4-dimethyl-3-oxopentane nitrile and 4-benzyloxyphenylhydrazine hydrochloride, using the same method as that described for preparation 7, as a pale pink powder in quantitative yield.

Workup

  1. customthat described for preparation 7, as a pale pink powder in quantitative yield

Sources & evidence

ORD record
ord-7ae1c945f3514849b65891563ac7b624
Source dataset
uspto-grants-2011_12
Patent number
US08076356B2

Reaction notes

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