HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxygen → 1-[3-(3,3-Dimethylbutoxy)-5-ethoxyphenyl]ethanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxygen | HCID 977 | — |
| Reactant | Cyclohexyl bromide | HCID 7960 | — |
| Reactant | 3',5'-Dihydroxyacetophenone | HCID 103993 | — |
| Reactant | 1-Bromo-3,3-dimethylbutane | HCID 137137 | — |
| Product | 1-[3-(3,3-Dimethylbutoxy)-5-ethoxyphenyl]ethanone | HCID 58136823 | — |
Reaction Steps
1-(3,5-Dihydroxyphenyl)ethanone (3.0 g) was converted analogously to O2.031. Instead of cyclohexylbromide, however, 1-bromo-3,3-dimethylbutane was used. After chromatography, 960 mg of the title compound were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08076336B2 |
| Source dataset | uspto-grants-2011_12 |
| ORD ID | ord-bba8b21f77754324b9d418114a0d3d1d |
| Source note | uspto-grants-2011_12 |