Benzamide → HCID 15173657, compound

HRID 657961Notes

Reaction equation

HRID 657961 reaction equation
[Br:1][C:2]1[CH:3]=[C:4]([CH:8]=[C:9]([O:13][CH3:14])[C:10]=1[O:11][CH3:12])[C:5]([OH:7])=O.[C:15](N)(=O)C1C=CC=CC=1>>[Br:1][C:2]1[CH:3]=[C:4]([C:5](=[O:7])[CH3:15])[CH:8]=[C:9]([O:13][CH3:14])[C:10]=1[O:11][CH3:12]

Participants

3

Reactant 2

HCID 2331BenzamideHCID 28181443-bromo-4,5-dimethoxybenzoic acid

Product 1

HCID 15173657HCID 15173657, compound

Procedure

3-Bromo-4,5-dimethoxybenzoic acid (2.0 g) was converted to the benzamide derivative analogously to O3.043, and the latter was converted to the title compound analogously to O2.059. 1.22 g of the title compound were obtained.

Sources & evidence

ORD record
ord-036bb1673b1e45f9b38b7f7a5a589c40
Source dataset
uspto-grants-2011_12
Patent number
US08076336B2

Reaction notes

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