HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromoethyl methyl ether → Methyl 3-tert-butyl-5-(2-methoxyethoxymethyl)benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromoethyl methyl ether | HCID 80972 | — |
| Reactant | Methyl 3-tert-butyl-5-(hydroxymethyl)benzoate | HCID 12144659 | — |
| Product | Methyl 3-tert-butyl-5-(2-methoxyethoxymethyl)benzoate | HCID 66941327 | — |
Reaction Steps
Methyl 3-tert-butyl-5-hydroxymethylbenzoate (6.0 g) was reacted analogously to O5.043 with 1-bromo-2-methoxyethane to give methyl 3-tert-butyl-5-(2-methoxyethoxymethyl)benzoate. The latter was then converted to the title compound analogously to the sequence O4.043 to O2.043. 508 mg of the title compound were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08076336B2 |
| Source dataset | uspto-grants-2011_12 |
| ORD ID | ord-518bb050329c4f57b74eccd2a2689ce4 |
| Source note | uspto-grants-2011_12 |